A gas-liq. chromatog. method is reported for detg. tricyclohexyltin hydroxide in powders marketed as insecticides, after its extn. with CHCl3. Different glass columns were tested using flame ionization or electron capture detectors. The linearity of the response was from 0.1 to 2.5 mg using the flame ionization detector and from 0.5 to 5.0 ng using the electron capture detector. Its recovery from the analyzed samples is satisfactory. Results of thermal anal., I.R. spectroscopy and mass spectrometry were also reported
Some chemical-physical properties of tricyclohexyltin hydroxide and its analytical determination / Camoni, I.; Chiacchierini, E.; Iachetta, R.; Magri', Antonio. - In: ANNALI DI CHIMICA. - ISSN 0003-4592. - STAMPA. - 65:5-6(1975), pp. 267-277.
Some chemical-physical properties of tricyclohexyltin hydroxide and its analytical determination
MAGRI', Antonio
1975
Abstract
A gas-liq. chromatog. method is reported for detg. tricyclohexyltin hydroxide in powders marketed as insecticides, after its extn. with CHCl3. Different glass columns were tested using flame ionization or electron capture detectors. The linearity of the response was from 0.1 to 2.5 mg using the flame ionization detector and from 0.5 to 5.0 ng using the electron capture detector. Its recovery from the analyzed samples is satisfactory. Results of thermal anal., I.R. spectroscopy and mass spectrometry were also reportedI documenti in IRIS sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.
