Radiofluorination of K arylpentafluorosilicates with AcO18F in AcOH gave 18F-labeled aryl fluorides in 6-20% yield. E.g., treatment of K2[4-MeC6H4SiF5] with AcO18F in AcOH at 25° for 10 min gave 18% 4-MeC6H418F.
Regiospecific radiofluorination of arylpentafluorosilicates as a general route to fluorine-18-labeled aryl fluorides / Speranza, Maurizio; C. Y., Shiue; A. P., Wolf; D. S., Wilbur; Angelini, Giancarlo. - In: JOURNAL OF THE CHEMICAL SOCIETY, CHEMICAL COMMUNICATIONS. - ISSN 0022-4936. - STAMPA. - 21(1984), pp. 1448-1449.
Regiospecific radiofluorination of arylpentafluorosilicates as a general route to fluorine-18-labeled aryl fluorides
SPERANZA, Maurizio;ANGELINI, Giancarlo
1984
Abstract
Radiofluorination of K arylpentafluorosilicates with AcO18F in AcOH gave 18F-labeled aryl fluorides in 6-20% yield. E.g., treatment of K2[4-MeC6H4SiF5] with AcO18F in AcOH at 25° for 10 min gave 18% 4-MeC6H418F.File allegati a questo prodotto
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