The structure of the title complex was detd. by Patterson and Fourier syntheses and refined by full-matrix least-squares to R = 0.059 for 1144 reflections. The compd. is monoclinic, space group P21/c, with a 19.166, b 11.235, c 14.191 Å, and β 103.1°; Z = 4. PdCl2L2 (L = R2C:NNMePh, R = Me, Et) and Pd2Cl4L2 (R = Et) were also prepd. and characterized by IR and NMR spectra.

Dimeric complexes of palladium with hydrazone. Crystal structure of bis(acetone methyl- phenylhydrazone) tetrachlorodipalladium(II) chloroform solvate (1:1) / M., BIAGINI CINGI; G., Natile; A., Tiripicchio; Gasparrini, Francesco. - In: JOURNAL OF CHEMICAL RESEARCH. SYNOPSES. - ISSN 0308-2342. - STAMPA. - (1979), pp. 98-99.

Dimeric complexes of palladium with hydrazone. Crystal structure of bis(acetone methyl- phenylhydrazone) tetrachlorodipalladium(II) chloroform solvate (1:1)

GASPARRINI, Francesco
1979

Abstract

The structure of the title complex was detd. by Patterson and Fourier syntheses and refined by full-matrix least-squares to R = 0.059 for 1144 reflections. The compd. is monoclinic, space group P21/c, with a 19.166, b 11.235, c 14.191 Å, and β 103.1°; Z = 4. PdCl2L2 (L = R2C:NNMePh, R = Me, Et) and Pd2Cl4L2 (R = Et) were also prepd. and characterized by IR and NMR spectra.
1979
01 Pubblicazione su rivista::01a Articolo in rivista
Dimeric complexes of palladium with hydrazone. Crystal structure of bis(acetone methyl- phenylhydrazone) tetrachlorodipalladium(II) chloroform solvate (1:1) / M., BIAGINI CINGI; G., Natile; A., Tiripicchio; Gasparrini, Francesco. - In: JOURNAL OF CHEMICAL RESEARCH. SYNOPSES. - ISSN 0308-2342. - STAMPA. - (1979), pp. 98-99.
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/11573/454410
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