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EnglishThe enantioselective behaviour of some underivatized 2-arylpropionic acids (profens) and flobufen by HPLC using a terguride-based chiral stationary phase was tested. X-ray analysis of crystals of the chiral selector and its complexes with naproxen allowed a deeper insight into the enantiodiscriminative process. The column stability and reproducibility, and the potential of the packing for semipreparative scale separations were also determined. A method for determining flobufen enantiomers and metabolites in plasma samples is described.
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| Titolo: | "Direct resolution of optically active isomers on chiral packings containing ergoline skeleton. 6. Enantioseparation of profens |
| Autori: | |
| Data di pubblicazione: | 1999 |
| Rivista: | |
| Abstract: | The enantioselective behaviour of some underivatized 2-arylpropionic acids (profens) and flobufen by HPLC using a terguride-based chiral stationary phase was tested. X-ray analysis of crystals of the chiral selector and its complexes with naproxen allowed a deeper insight into the enantiodiscriminative process. The column stability and reproducibility, and the potential of the packing for semipreparative scale separations were also determined. A method for determining flobufen enantiomers and metabolites in plasma samples is described. |
| Handle: | http://hdl.handle.net/11573/33746 |
| Appare nella tipologia: | 01a Articolo in rivista |
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